Amazing Spider-Man #66 Nov 1968
"The Madness of Mysterio!"
Mysterio has broken out of prison and is using his special effects prowess to prepare another plot to get revenge against Spider-Man;
Meanwhile, Spidey recovers his clothes and camera left in the debris following his fight with the Vulture;
The next day he tries to sell the pictures to Jameson; Furious that Parker "abandoned" him when he was supposed to be taking pictures
of Spider-Man's battle with the Vulture, he throws Parker out of the building, telling Peter that he doesn't need him to take pictures;
Appearing on television, Mysterio issues a challenge to Spider-Man to meet him to a fight to the finish or he will start destroying city bridges.
Script by Stan Lee,
pencils by John Romita Sr. (layouts) and Don Heck (pencils),
inks by Mike Esposito (as Mickey Demeo)